HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
3-Phenylprop-2-Enal → HCID 20067707, Verbindung
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 3-Phenylprop-2-Enal | HCID 307 | — |
| Edukt | 4-Benzyloxybenzophenone | HCID 458193 | — |
| Produkt | HCID 20067707 | HCID 20067707 | — |
Reaktionsschritte
The (RR,SS; RS,SR)-isomer mixture is prepared from 13.2 g of cinnamaldehyde and 28.8 g of 4-benzyloxybenzophenone according to the procedure described in Example 9. Recrystallization is performed from toluene. The yield is 32.5 g (77%) of a product having m.p. 109°-15° C. The product contains both isomer pairs (RR,SS: RS,SR 1:1).
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US04996225 |
| Quelldatensatz | uspto-grants-1991_02 |
| ORD ID | ord-ef7c29f058d74ec0800ee44b30bb37e6 |
| Quellennotiz | uspto-grants-1991_02 |