Acetone → 2,6-Dihydroxynaphthalene

HRID 982562

Reaktionsgleichung

[CH3:1][C:2]([CH3:4])=[O:3].[CH3:5][CH:6]([CH2:8][C:9]([CH3:11])=[O:10])[CH3:7].[CH3:12]C(C)=O>>[OH:3][C:2]1[CH:4]=[CH:7][C:6]2[C:5](=[CH:12][CH:11]=[C:9]([OH:10])[CH:8]=2)[CH:1]=1

Komponenten

Edukt 2

HCID 180Acetone

HCID 18671121MIBK acetone

Produkt 1

HCID 935522,6-Dihydroxynaphthalene

Versuchsvorschrift

Sixty parts by weight of acetone was added to 100 parts by weight of the oily phase containing the oxidation product obtained in Example 8, (1) to prepare an MIBK/acetone mixed oily phase which was subjected to acid cleavage by the following method to obtain 2,6-dihydroxynaphthalene.

Quellen und Nachweise

ORD-Eintrag: ord-c8d800a2a68e4214a68488536c41fcff
Quelldatensatz: uspto-grants-1991_02
DOI: 10.6084/m9.figshare.5104873.v1
Patentnummer: US04996372

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