Malononitrile, benzylidene- → 5-Aminomethyl-2-(3,4-dimethoxy-phenyl)-6-phenyl-pyrimidin-4-ylamine

HRID 983873

Reaktionsgleichung

Reaktionsgleichung von HRID 983873
[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][C:11]=1[O:12][CH3:13])[C:6]([NH2:8])=[NH:7].[CH:14](=[C:21]([C:24]#[N:25])[C:22]#[N:23])[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1>>[NH2:25][CH2:24][C:21]1[C:22]([NH2:23])=[N:7][C:6]([C:5]2[CH:9]=[CH:10][C:11]([O:12][CH3:13])=[C:3]([O:2][CH3:1])[CH:4]=2)=[N:8][C:14]=1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1

Komponenten

3

Edukt 2

HCID 17608Malononitrile, benzylidene-HCID 40034Benzenecarboximidamide, 3,4-dimethoxy-

Produkt 1

HCID 102153045-Aminomethyl-2-(3,4-dimethoxy-phenyl)-6-phenyl-pyrimidin-4-ylamine

Versuchsvorschrift

The title compound, MS: m/e=336.8 (M+H+), was prepared from 3,4-dimethoxybenzamidine and 2-benzylidene-malononitrile in analogy to the process described in Example 11 as a solid.

Quellen und Nachweise

ORD-Eintrag
ord-8b39335753224af9a64a100adc6e9072
Quelldatensatz
uspto-grants-2005_03
Patentnummer
US06867205B2

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