Potassium Carbonate → HCID 19858315, Verbindung

HRID 985962Notizen

Reaktionsgleichung

Reaktionsgleichung von HRID 985962
[CH3:1][O:2][CH:3]=[CH:4]C.[I:6][CH2:7][CH2:8][OH:9].[C:10](=O)([O-])[O-].[K+].[K+]>P(Cl)(Cl)(Cl)=O>[CH3:1][O:2][C:3]([O:9][CH2:8][CH2:7][I:6])([CH3:4])[CH3:10]

Komponenten

5

Edukt 3

HCID 11430Potassium CarbonateHCID 12225IodoethanolHCID 1112901-Propene, 1-methoxy-

Produkt 1

HCID 19858315HCID 19858315, Verbindung

Reagenzien, Katalysatoren, Lösungsmittel 1

HCID 24813Phosphorus oxychlorideKatalysator

Versuchsvorschrift

To 6 mls of cold (0° C.) methoxypropene was added 3 mls of 2-iodoethanol and 1 drop of phosphorous oxychloride (POCl3). The reaction was stirred for 1 hour and then solid potassium carbonate was added. After 10 minutes the liquid was decanted and concentrated to give the product as an oil.

Aufarbeitung

  1. customAfter 10 minutes the liquid was decanted
  2. concentrationconcentrated

Quellen und Nachweise

ORD-Eintrag
ord-c08d7a259d0748bf9a260847ae432013
Quelldatensatz
uspto-grants-1987_12
Patentnummer
US04710504

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