2,6-Di-tert-butyl-4-mercaptophenol → HCID 14011803, Verbindung
Reaktionsgleichung
Cl[CH2:2][CH2:3][S:4]([CH2:7][C:8]([O:10][CH3:11])=[O:9])(=[O:6])=[O:5].[O-][CH2:13]C.[Na+].[CH3:16][C:17]([C:20]1[CH:25]=[C:24]([SH:26])[CH:23]=[C:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:21]=1[OH:31])([CH3:19])[CH3:18]>>[CH3:19][C:17]([C:20]1[CH:25]=[C:24]([S:26][CH2:2][CH2:3][S:4]([CH2:7][C:8]([O:10][CH2:11][CH3:13])=[O:9])(=[O:6])=[O:5])[CH:23]=[C:22]([C:27]([CH3:30])([CH3:29])[CH3:28])[C:21]=1[OH:31])([CH3:16])[CH3:18]Komponenten
4
Versuchsvorschrift
The title compound was prepared according to the method of Example 12 from the title compound of Example 16, sodium ethoxide and 2,6-bis(1,1-dimethylethyl)-4-mercaptophenol, m.p. ca. 95° C.
Quellen und Nachweise
- ORD-Eintrag
- ord-7651419618ce4c1a808f0b74d7ecf79d
- Quelldatensatz
- uspto-grants-1987_12