HuagongsheHuagongshe Chemie-Druckbericht · Nur für Forschungszwecke
4-Methoxybenzenethiol → 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester
Beteiligte Stoffe
| Rolle | Name | HCID | Einwaage |
|---|---|---|---|
| Edukt | 4-Methoxybenzenethiol | HCID 12765 | — |
| Edukt | Ethyl 2-bromoheptanoate | HCID 95333 | — |
| Produkt | 2-(4-Methoxy-phenylsulfanyl)heptanoic acid ethyl ester | HCID 54357246 | 108,8% |
Reaktionsschritte
2-(4-Methoxy-phenylsulfanyl)-heptanoic acid ethyl ester (13.8 g, 98%) was prepared according to the general method as outlined in example 1 starting from ethyl 2-bromoheptanoate (11 g, 47 mmol) and 4-methoxythiophenol (6 g, 42.8 mmol), as a yellow oil; MS: 297.2 (M+H)+.
Herkunft & Nachweise
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patentnummer | US06462073B2 |
| Quelldatensatz | uspto-grants-2002_10 |
| ORD ID | ord-a24c4c085352445a978f1232c59e598c |
| Quellennotiz | uspto-grants-2002_10 |