O-Benzylhydroxylamine → 4-(O-Benzylhydroxylamino)-3-chloro-2-ethylpyridine
Reaction equation
[Cl:1][C:2]1[C:3]([CH2:9][CH3:10])=[N:4][CH:5]=[CH:6][C:7]=1Cl.[CH2:11]([O:18][NH2:19])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1>>[CH2:11]([O:18][NH:19][C:7]1[CH:6]=[CH:5][N:4]=[C:3]([CH2:9][CH3:10])[C:2]=1[Cl:1])[C:12]1[CH:17]=[CH:16][CH:15]=[CH:14][CH:13]=1Participants
3
Procedure
Preparation was carried out analogously to Example 1 from 3,4-dichloro-2-ethylpyridine and O-benzylhydroxylamine. Yield: 99%
Workup
- customPreparation
Sources & evidence
- ORD record
- ord-cf5b984642ac4823a3cc135bcd09ba2e
- Source dataset
- uspto-grants-1998_03
- Patent number
- US05723450
Reaction notes
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