HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diisopropyl Ether → HCID 178418452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diisopropyl Ether | HCID 7914 | — |
| Reactant | 4-(2,4,4-Trimethylpentan-2-yl)cyclohexan-1-one | HCID 19693931 | — |
| Reactant | 4-Ethyl-4-amino-5-bromopyridine | HCID 67670297 | — |
| Product | HCID 178418452 | HCID 178418452 | — |
Reaction Steps
As Example 75, but using 2.01 g (10 mmol) of 4-ethyl-4-amino-5-bromopyridine instead of 2-ethyl-3-bromo-4-aminopyridine and 4.2 g (20 mmol) of 4-(1,1,3,3-tetramethylbutyl)cyclohexanone instead of 4-phenylcyclohexanone. Yield: 1.9 g (48%); Rf =0.39 (diisopropyl ether)
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723450 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-bbef73e40290461c80e983d0e34bab95 |
| Source note | uspto-grants-1998_03 |