Potassium Hydroxide → HCID 19901125, compound
Reaction equation
[S:1]1[CH2:4][S:3][C:2]1=[C:5]([C:11]([O:13]CC)=[O:12])[C:6]([O:8][CH2:9][CH3:10])=[O:7].[OH-].[K+]>C(O)C>[S:1]1[CH2:4][S:3][C:2]1=[C:5]([C:11]([OH:13])=[O:12])[C:6]([O:8][CH2:9][CH3:10])=[O:7]Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
Diethyl 2-(1,3-dithietan-2-ylidene)malonate was treated with a solution of potassium hydroxide in ethanol. The resultant solid was isolated and purified by the same method as in Example 1 to afford the titled compound as a white solid. (51%).
Workup
- customThe resultant solid was isolated
- custompurified by the same method as in Example 1
Sources & evidence
- ORD record
- ord-192d02d1cbd44f0e857d2f19aac69229
- Source dataset
- uspto-grants-1992_04
- Patent number
- US05103013
Reaction notes
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