HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methyl bromoacetate → Methyl (2-formyl-4-methoxyphenoxy)acetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methyl bromoacetate | HCID 60984 | — |
| Reactant | 2-Hydroxy-5-methoxybenzaldehyde | HCID 95695 | — |
| Product | Methyl (2-formyl-4-methoxyphenoxy)acetate | HCID 43212883 | 86% |
Reaction Steps
In the same manner as in Reference Example 1, 5-methoxysalicylaldehyde was reacted with methyl bromoacetate to yield methyl 2-formyl-4-methoxyphenoxyacetate (yield 86%), which was then recrystallized from acetone-hexane to yield colorless prisms having a melting point of 74° to 75° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723479 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-8d8d9084812145079c62beccf28cf5f0 |
| Source note | uspto-grants-1998_03 |