Reaction equation
[CH3:1][Sn](C)(C)C.[OH:6][C:7]1[C:16]2[C:11](=[C:12]([NH2:17])[CH:13]=[CH:14][CH:15]=2)[C:10](Br)=[CH:9][N:8]=1>>[OH:6][C:7]1[C:16]2[C:11](=[C:12]([NH2:17])[CH:13]=[CH:14][CH:15]=2)[C:10]([CH3:1])=[CH:9][N:8]=1Participants
3
Procedure
According to the method of Example 106, Step A, a methylation reaction with tetramethyltin was performed by using Intermediate 138 to obtain the title compound.
Sources & evidence
- ORD record
- ord-6c378cc1f8624b089d5efbafe5b55132
- Source dataset
- uspto-grants-2006_08
- Patent number
- US07094789B2
Linked notes
Loading…