HCID 22280189, compound → 2,5-Dimethyl-4-thiocyanato-phenol

Reaction equation

COC1C(SC#N)=CC(C)=C(O)C=1.COC(=O)C[O:18][C:19]1[CH:24]=[C:23]([CH3:25])[C:22]([S:26][C:27]#[N:28])=[CH:21][C:20]=1[CH3:29]>>[CH3:29][C:20]1[CH:21]=[C:22]([S:26][C:27]#[N:28])[C:23]([CH3:25])=[CH:24][C:19]=1[OH:18]

Participants

Reactant 2

HCID 22280189HCID 22280189, compound

HCID 85845775HCID 85845775, compound

Product 1

HCID 222800452,5-Dimethyl-4-thiocyanato-phenol

Procedure

The title compound was prepared in a manner analogous to compound 1B. 400 MHz 1H NMR (DMSO-d6) δ 10.0 (s, 1H), 7.35 (s, 1H), 6.73 (s, 1H), 2.3 (s, 3H), 2.04 (s, 3H); MS m/z 180 (m+1). Preparation of (2,5-Dimethyl-4-thiocyanato-phenoxy)-acetic acid methyl ester (Compound WWB)

Sources & evidence

ORD record: ord-25031e1a76204c62ade45b72b495a53f
Source dataset: uspto-grants-2005_11
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06964983B2

Reaction notes

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