HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetic Acid → Dodecanedioic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetic Acid | HCID 176 | — |
| Reactant | Cyclododecene, (E)- | HCID 15164 | — |
| Reactant | 3a,4,5,7a-Tetrahydro-2-benzofuran-1,3-dione | HCID 12726601 | — |
| Product | Dodecanedioic Acid | HCID 12736 | 94% |
Reaction Steps
The co-oxidation reaction was carried out in a manner as described in Example 1, except that cyclododecene was used in lieu of cis-Δ4 -tetrahydrophthalic anhydride. Acetic acid was obtained at a yield of 95% and 1,10-dicarboxy decane was obtained at a yield of 94%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04331608 |
| Source dataset | uspto-grants-1982_05 |
| ORD ID | ord-c134627c84a54450bdb1e8d5cc547349 |
| Source note | uspto-grants-1982_05 |