3-Nitrophenylboronic Acid → HCID 16125934, compound

HRID 1069075

Reaction equation

HRID 1069075 reaction equation
[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][N:9]=[C:8](Br)[CH:7]=1)=[O:5])[CH3:2].[N+:13]([C:16]1[CH:17]=[C:18](B(O)O)[CH:19]=[CH:20][CH:21]=1)([O-:15])=[O:14]>>[CH2:1]([O:3][C:4]([C:6]1[CH:11]=[CH:10][N:9]=[C:8]([C:20]2[CH:19]=[CH:18][CH:17]=[C:16]([N+:13]([O-:15])=[O:14])[CH:21]=2)[CH:7]=1)=[O:5])[CH3:2]

Participants

3

Reactant 2

HCID 16773-Nitrophenylboronic AcidHCID 3847769Ethyl 2-bromoisonicotinate

Product 1

HCID 16125934HCID 16125934, compound

Procedure

Electrospray MS (positive ion): (M+H) 272.8; from 2-bromo4-pyridinecarboxylic acid ethyl ester (900 mg), tetrakis(triphenylphosphine)paliadium (136 mg), and 3-nitrophenylboronic acid (783 mg).

Sources & evidence

ORD record
ord-27722b9457f94597a2204c9f2a93a4fc
Source dataset
uspto-grants-2001_06
Patent number
US06251925B1

Linked notes

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