HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium sulfate → Glucosamine sulfate lithium chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium sulfate | HCID 66320 | — |
| Reactant | (3R,4R,5S,6R)-3-amino-6-(hydroxymethyl)oxane-2,4,5-triol hydrochloride | HCID 2723635 | — |
| Solvent | Water | HCID 962 | — |
| Product | Glucosamine sulfate lithium chloride | HCID 86754062 | — |
Reaction Steps
Example 1 was repeated using 1679 g of purified water, 431.5 g (2 moles) of glucosamine hydrochloride and 128 g (1 mole) of lithium sulfate (monohydrate) instead of the sodium sulfate. After freeze drying, glucosamine sulfate lithium chloride was obtained as a white powder in a yield of 525 g (97% of theoretical).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05902801 |
| Source dataset | uspto-grants-1999_05 |
| ORD ID | ord-936ee2068b904d9798f028b3ea0fbb36 |
| Source note | uspto-grants-1999_05 |