Dimethylamine → HCID 21536680, compound
Reaction equation
CNC.[Br:4][C:5]1[C:6]([CH3:17])=[N:7][N:8]([CH:11]([CH2:15][CH3:16])[C:12]([OH:14])=O)[C:9]=1[CH3:10].BrC1[C:23](Br)=[C:22](C)[N:21]([CH:26](C)[C:27](O)=O)N=1>>[Br:4][C:5]1[C:6]([CH3:17])=[N:7][N:8]([CH:11]([CH2:15][CH3:16])[C:12]([N:21]([CH2:26][CH3:27])[CH2:22][CH3:23])=[O:14])[C:9]=1[CH3:10]Participants
4
Procedure
Following the procedure of Example 1, Part C, but substituting diethylamine for dimethylamine and further substituting the 4-bromo-α-ethyl-3,5-dimethylpyrazole-1-acetic acid prepared in Example 60, Part B, above, for the 3,4-dibromo-α,5-dimethylpyrazole-1-acetic acid, there was prepared the corresponding 4-bromo-N,Nα-triethyl-3,5-dimethylpyrazole-1-acetamide having a melting point at 42° to 44° C.
Sources & evidence
- ORD record
- ord-5572e46a5aaf41c4a51d40667ffee382