p-Fluoronitrobenzene → HCID 21625360, compound

HRID 1085265

Reaction equation

HRID 1085265 reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[CH3:11][NH:12][CH2:13][CH2:14][N:15]([CH3:20])[CH2:16][CH2:17][NH:18][CH3:19]>CS(C)=O>[CH3:11][N:12]([C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1)[CH2:13][CH2:14][N:15]([CH3:20])[CH2:16][CH2:17][NH:18][CH3:19]

Participants

4

Reactant 2

HCID 9590p-FluoronitrobenzeneHCID 669301,4,7-Trimethyldiethylenetriamine

Product 1

HCID 21625360HCID 21625360, compound

Reagents, catalysts & solvents 1

HCID 679Dimethyl SulfoxideSolvent

Conditions

Temperature
120 °C

Procedure

In 7 ml of dimethyl sulfoxide were dissolved 1.41 g of p-fluoronitrobenzene and 14 g of N,N',N"-trimethyldiethylenetriamine, and the mixture was then stirred at 120° C. for 3 hours.

Sources & evidence

ORD record
ord-ea800a3811824a62a5c3612ba298168a
Source dataset
uspto-grants-1991_04
Patent number
US05008267

Linked notes

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