1,5-Dibromopentane → HCID 20062139, compound

HRID 1085380

Reaction equation

HRID 1085380 reaction equation
[CH2:1]([O:19][CH2:20][CH2:21][CH2:22][OH:23])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[Br:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29]Br.[OH-].[Na+]>[Cl-].C([N+](C)(C)C)CCCCCCCCCCCCCCC>[Br:24][CH2:25][CH2:26][CH2:27][CH2:28][CH2:29][O:23][CH2:22][CH2:21][CH2:20][O:19][CH2:1][CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8][CH2:9][CH2:10][CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

5

Reactant 3

HCID 81001,5-DibromopentaneHCID 14798Sodium HydroxideHCID 5553033-Octadecyloxypropanol

Product 1

HCID 20062139HCID 20062139, compound

Reagents, catalysts & solvents 1

HCID 8154Hexadecyltrimethylammonium chlorideCatalyst

Procedure

Employing 3-(octadecyloxy)propanol (5 g), 1,5-dibromopentane (10.8 g), cetyltrimethylammonium chloride (0.96 g) and a 50% aqueous solution of sodium hydroxide (12 g), a reaction and aftertreatment are conducted in the same manner as those in Reference Example 4 to obtain the above-titled compound as colorless wax (3.75 g).

Sources & evidence

ORD record
ord-8155d98e9e2d40e28d0276e3cecbe98d
Source dataset
uspto-grants-1991_04
Patent number
US05008454

Linked notes

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