HuagongsheHuagongshe Chemistry Print Report · For research reference only
Epichlorohydrin → 3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropane
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Epichlorohydrin | HCID 7835 | — |
| Reactant | 1-Bromo-2-naphthol | HCID 11316 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Solvent | Methyl Ethyl Ketone | HCID 6569 | — |
| Product | 3-(1-Bromonaphth-2-yloxy)-1,2-epoxypropane | HCID 14369942 | — |
Reaction Steps
A suspension containing 22.3 g of 1-bromonaphth-2-ol, 27.75 g of 1-chloro-2,3-epoxypropane and 27.6 g of potassium carbonate in 200 ml of butanone is refluxed overnight. The inorganic salts are filtered off and drained and the filtrate is then evaporated under vacuum. The oil obtained is distilled under 0.01 mm of mercury.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05036077 |
| Source dataset | uspto-grants-1991_07 |
| ORD ID | ord-e743b44489f04654891d9a3d50b33511 |
| Source note | uspto-grants-1991_07 |