HCID 57426190, compound → HCID 57426221, compound

Reaction equation

[C:1]([CH2:3][C:4]1[C:12]2[C:7](=[CH:8][CH:9]=[CH:10][C:11]=2[N+:13]([O-:15])=[O:14])[N:6](CC(OC(C)(C)C)=O)[CH:5]=1)#[N:2].[CH:24](C1NC2C(C=1)=C([N+]([O-])=O)C=CC=2)([CH3:26])[CH3:25]>>[CH:24]([C:5]1[NH:6][C:7]2[C:12]([C:4]=1[CH2:3][C:1]#[N:2])=[C:11]([N+:13]([O-:15])=[O:14])[CH:10]=[CH:9][CH:8]=2)([CH3:26])[CH3:25]

Participants

Reactant 2

HCID 57426190HCID 57426190, compound

HCID 57426220HCID 57426220, compound

Product 1

HCID 57426221HCID 57426221, compound

Procedure

Essentially following the procedures described for Intermediate 11, but using 2-isopropyl-4-nitro-1H-indole from Step B in place of 4-nitroindole, the title compound was prepared. MS: m/z=244 (M+1).

Sources & evidence

ORD record: ord-cff5fd6f1a7b4f8d8654d6b62308e1cb
Source dataset: uspto-grants-2012_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08133891B2

Reaction notes

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