HuagongsheHuagongshe Chemistry Print Report · For research reference only
Benzyl Alcohol → 7-Benzyloxy-1-(2-butenyl)-2,3-dimethylpyrrolo[2,3-d]pyridazine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Benzyl Alcohol | HCID 244 | — |
| Reactant | 1-(2-Butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53719624 | — |
| Product | 7-Benzyloxy-1-(2-butenyl)-2,3-dimethylpyrrolo[2,3-d]pyridazine | HCID 53656015 | 78.6% |
Reaction Steps
The title compound (cis/trans=21/79) was prepared as pale brown crystals in 78.6 % yield in a similar procedure to that described in Example 1 by using 1-(2-butenyl)-7-chloro-2,3-dimethylpyrrolo[2,3-d]pyridazine [cis/trans (18/82)] and benzyl alcohol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06063782 |
| Source dataset | uspto-grants-2000_05 |
| ORD ID | ord-b75ebdde71a84a9abb646b9bf22a5f04 |
| Source note | uspto-grants-2000_05 |