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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1108536Generated: October 23, 2026

H acid → 1-Hydroxy-8-(2,4-dichloro-s-triazin-6-ylamino-)naphthalene-3,6-disulphonic acid

https://huagongshe.com/en/reaction/1108536

Reaction equation

Participants

RoleNameHCIDCharge
ReactantH acidHCID 7009—
ReactantCyanuric chlorideHCID 7954—
SolventWaterHCID 962—
Product1-Hydroxy-8-(2,4-dichloro-s-triazin-6-ylamino-)naphthalene-3,6-disulphonic acidHCID 11048924—

Reaction Conditions

Temperature2.5 °C

Reaction Steps

An ice cold neutral solution of 1-hydroxy-8-aminonaphthalene-3,6-disulphonic acid (31.9 parts) in water (120 parts) was added, with stirring, to a freshly prepared suspension of 2,4,6-trichloro-s-triazine (18.5 parts) in ice and water (140 parts). The mixture was stirred for 3 hours at 0 to 5° C. to give a solution of 1-hydroxy-8-(2,4-dichloro-s-triazin-6-ylamino-)naphthalene-3,6-disulphonic acid (solution 1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS06068667
Source datasetuspto-grants-2000_05
ORD IDord-96c6ea8add314387a32fb0ab620e9b4d
Source noteuspto-grants-2000_05