Cesium fluoride → Allyl Oxalofluoride

HRID 1109259

Reaction equation

HRID 1109259 reaction equation
[CH2:1]([O:4][C:5](=[O:9])[C:6](Cl)=[O:7])[CH:2]=[CH2:3].[F-:10].[Cs+]>>[CH2:1]([O:4][C:5](=[O:9])[C:6]([F:10])=[O:7])[CH:2]=[CH2:3]

Participants

3

Reactant 2

HCID 25953Cesium fluorideHCID 3018516Allyl chlorooxoacetate

Product 1

HCID 14153244Allyl Oxalofluoride

Procedure

By the procedure of the preceding Preparation, allyl oxalochloride (252.5 g, 1.70 mol) and cesium fluoride (284 g, 1.87 mol) were converted to twice distilled title product, b.p. 48°-50° C./35 mm; 124°-126° C. (atmospheric pressure).

Workup

  1. distillationto twice distilled title product, b.p. 48°-50° C./35 mm
  2. custom124°-126° C. (atmospheric pressure)

Sources & evidence

ORD record
ord-f50bba0a23a44a65b38e743dc1911933
Source dataset
uspto-grants-1994_06
Patent number
US05319103

Linked notes

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