9-Octadecenoic Acid → 9-Octadecenoyl chloride

Reaction equation

C(O)(=O)CCCCCCCC=CCCCCCCCC.[C:21]([Cl:40])(=[O:39])[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH:29]=[CH:30][CH2:31][CH:32]=[CH:33][CH2:34][CH2:35][CH2:36][CH2:37][CH3:38]>>[C:21]([Cl:40])(=[O:39])[CH2:22][CH2:23][CH2:24][CH2:25][CH2:26][CH2:27][CH2:28][CH:29]=[CH:30][CH2:31][CH2:32][CH2:33][CH2:34][CH2:35][CH2:36][CH2:37][CH3:38]

Participants

Reactant 2

HCID 9659-Octadecenoic Acid

HCID 98987Octadeca-9,12-dienoyl chloride

Product 1

HCID 669879-Octadecenoyl chlorideYield 85%

Procedure

Octadec-9-enoyl chloride (25.5 parts, boiling point 160°-180° C. at 0.12 Torr, 85% yield) was prepared from 28.1 parts of octadec-9-enoic acid using the procedure described in part A of Example 3 for the preparation of octadec-9,12-dienoyl chloride.

Sources & evidence

ORD record: ord-6d5a70a1d0b84c97a29c84fa2615f05a
Source dataset: uspto-grants-1990_12
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US04978756

Reaction notes

Loading…