HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Fluorobenzyl bromide → 7-(1-Adamantyl)-6-(4-fluorobenzyl)oxy-2-bromonaphthalene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Fluorobenzyl bromide | HCID 68021 | — |
| Reactant | 3-(Adamantan-1-yl)-6-bromonaphthalen-2-ol | HCID 14549072 | — |
| Product | 7-(1-Adamantyl)-6-(4-fluorobenzyl)oxy-2-bromonaphthalene | HCID 22000379 | 86% |
Reaction Steps
Following the basic procedure of Example 11, by reacting 1.1 g (3 mmol) of 7-(1-adamantyl)-6-hydroxy-2-bromonaphthalene with 420 μl (3,3 mmol) of 4-fluorobenzyl bromide, 1.2 g (86%) of the expected compound was obtained in the form of a colorless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723499 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-f03bd0e627354ee4a55f5536f5f04cf4 |
| Source note | uspto-grants-1998_03 |