Zirconium(IV) propoxide → HCID 86738105, compound

HRID 1155180Notes

Reaction equation

HRID 1155180 reaction equation
C[Si]([O:5][P:6]([CH2:13][CH2:14][CH2:15][CH2:16][C:17]([O:19][CH2:20][CH3:21])=[O:18])(=[O:12])[O:7][Si](C)(C)C)(C)C.[O-]CCC.[Zr+4:26].[O-]CCC.[O-]CCC.[O-]CCC>>[Zr:26].[C:17]([CH2:16][CH2:15][CH2:14][CH2:13][P:6](=[O:5])([O-:12])[O-:7])([O:19][CH2:20][CH3:21])=[O:18]

Participants

3

Reactant 2

HCID 90139Zirconium(IV) propoxideHCID 20562960Bis-trimethylsilyl-4-carboethoxybutylphosphonate

Product 1

HCID 86738105HCID 86738105, compound

Procedure

To a reaction flask under an inert atmosphere was added 3.13 g of bis-trimethylsilyl-4-carboethoxybutylphosphonate. To the flask was slowly added 1.44 g of zirconium propoxide. After the first few drops were added, a gelatinous product was formed. Agitation was continued during the remainder of the addition.

Workup

  1. additionAfter the first few drops were added
  2. customa gelatinous product was formed
  3. additionAgitation was continued during the remainder of the addition

Sources & evidence

ORD record
ord-45ed4196492f405b81404d672065348d
Source dataset
uspto-grants-1981_11
Patent number
US04299943

Reaction notes

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