HuagongsheHuagongshe Chemistry Print Report · For research reference only
Azobisisobutyronitrile → Phenyl 2-methoxy-3-bromomethylphenyl ether
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Azobisisobutyronitrile | HCID 6547 | — |
| Reactant | N-bromobutanimide | HCID 67184 | — |
| Reactant | Phenyl 2-methoxy-3-methylphenyl ether | HCID 20082997 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | Phenyl 2-methoxy-3-bromomethylphenyl ether | HCID 20513501 | 103.5% |
Reaction Steps
A mixture of phenyl 2-methoxy-3-methylphenyl ether (6 g), N-bromosuccinimide (5.2 g) and azobisisobutyronitrile (500 mg) in dried benzene (60 ml) was treated in a similar manner to that of Example 14-(3) to give oily phenyl 2-methoxy-3-bromomethylphenyl ether (8.5 g).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04367238 |
| Source dataset | uspto-grants-1983_01 |
| ORD ID | ord-9585e5e9803040eeb09a1d3008e26a77 |
| Source note | uspto-grants-1983_01 |