HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trehalose, dihydrate → Trehalose
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trehalose, dihydrate | HCID 181978 | — |
| Solvent | Water | HCID 962 | — |
| Product | Trehalose | HCID 7427 | 20% |
Reaction Steps
Trehalose dihydrate was dissolved in demineralised water to give a 20% trehalose solution. The solution was frozen to −40° C., then freeze dried in an Edwards freeze dryer. A powdered material typical of freeze dried powder was obtained. The material was confirmed to be completely amorphous by DSC and X-ray powder diffraction.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06620791B1 |
| Source dataset | uspto-grants-2003_09 |
| ORD ID | ord-0c991057eca14898812b21f6f22e2087 |
| Source note | uspto-grants-2003_09 |