Ethanolamine → 2-(4-Nitroanilino)ethanol
Reaction equation
F[C:2]1[CH:7]=[CH:6][C:5]([N+:8]([O-:10])=[O:9])=[CH:4][CH:3]=1.[NH2:11][CH2:12][CH2:13][OH:14]>>[N+:8]([C:5]1[CH:6]=[CH:7][C:2]([NH:11][CH2:12][CH2:13][OH:14])=[CH:3][CH:4]=1)([O-:10])=[O:9]Participants
3
Procedure
The title compound was prepared from 1-fluoro-4-nitrobenzene and 2-aminoethanol following the procedure described above. MS (ES+): m/z=183.0; 1H NMR (CDCl3, 500 MHz): δ 3.41 (t, 2H), 3.92 (t, 2H), 6.59 (d, 2H), 8.11 (d, 2H).
Sources & evidence
- ORD record
- ord-fea5d066ded645f1a967205c94b001a3
- Source dataset
- uspto-grants-2007_10
- Patent number
- US07279469B2
Reaction notes
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