m-Anisoyl chloride → HCID 178490483, compound

Reaction equation

[CH3:1][O:2][C:3]1[CH:4]=[C:5]([CH:9]=[CH:10][CH:11]=1)[C:6](Cl)=[O:7].ClC1C=CC(C([NH:19][C:20]2[CH:21]=[N:22][C:23]([OH:26])=[CH:24][CH:25]=2)=O)=CC=1>>[OH:26][C:23]1[N:22]=[CH:21][C:20]([NH:19][C:6](=[O:7])[C:5]2[CH:9]=[CH:10][CH:11]=[C:3]([O:2][CH3:1])[CH:4]=2)=[CH:25][CH:24]=1

Participants

Reactant 2

HCID 74374m-Anisoyl chloride

HCID 178522254HCID 178522254, compound

Product 1

HCID 178490483HCID 178490483, compound

Procedure

Starting from 3-methoxybenzoyl chloride (1.71 g, 10.0 mmol) and using the procedure as described for the preparation of 4-Chloro-N-(6-hydroxy-pyridin-3-yl)-benzamide yielded the title compound, which was used without further purification.

Sources & evidence

ORD record: ord-40177707347c4ef09e4f34a3ef77dc75
Source dataset: uspto-grants-2007_10
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07279470B2

Reaction notes

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