Carbamic chloride, N-methyl-N-phenyl- → HCID 10286262, compound
Reaction equation
[OH:1][N:2]1[CH:6]=[C:5]([Br:7])[CH:4]=[N:3]1.[CH3:8][N:9]([C:13]1[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=1)[C:10](Cl)=[O:11]>CCOC(C)=O.CCCCCCC>[Br:7][C:5]1[CH:4]=[N:3][N:2]([O:1][C:10](=[O:11])[N:9]([CH3:8])[C:13]2[CH:18]=[CH:17][CH:16]=[CH:15][CH:14]=2)[CH:6]=1Participants
4
Reactant 2
Product 1
Reagents, catalysts & solvents 1
Procedure
The title compound was prepared from 1-hydroxy-4-bromopyrazole and N-methyl-N-phenylcarbamoyl chloride. The crude product was subjected to flash chromatography (Quad flash 25, EtOAc-heptane) (89%, oil). HPLC-MS m/z=298.0 (M+1), Rt: 3.77 min.
Sources & evidence
- ORD record
- ord-a6c315395ea44d42a93debbe5f910e3a
- Source dataset
- uspto-grants-2007_10
- Patent number
- US07279470B2
Reaction notes
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