Aniline → N-phenyl-2-Dibenzofuranamine

HRID 1183195Notes

Reaction equation

HRID 1183195 reaction equation
I[C:2]1[CH:14]=[CH:13][C:5]2[O:6][C:7]3[CH:12]=[CH:11][CH:10]=[CH:9][C:8]=3[C:4]=2[CH:3]=1.[NH2:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1>C(OCC)(=O)C.CCCCCC>[CH:3]1[C:4]2[C:8]3[CH:9]=[CH:10][CH:11]=[CH:12][C:7]=3[O:6][C:5]=2[CH:13]=[CH:14][C:2]=1[NH:15][C:16]1[CH:21]=[CH:20][CH:19]=[CH:18][CH:17]=1

Participants

4

Reactant 2

HCID 6115AnilineHCID 2233272-Iododibenzofuran

Product 1

HCID 67204676N-phenyl-2-Dibenzofuranamine

Reagents, catalysts & solvents 1

HCID 21226206Ethyl acetate hexaneSolvent

Procedure

The Rf values of the object of the synthesis, 2-iododibenzofuran, and aniline were respectively 0.28, 0.59, and 0.07, which were found by silica gel thin layer chromatography (TLC) (ethyl acetate:hexane (1:10) as the developing solvent).

Sources & evidence

ORD record
ord-b4025fc9e8914b338ad9ffe16113d389
Source dataset
uspto-grants-2014_03
Patent number
US08664263B2

Reaction notes

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