Adipic Acid → 1-Ethyl hexanedioate

HRID 1192843

Reaction equation

[C:1]([OH:10])(=[O:9])[CH2:2][CH2:3][CH2:4][CH2:5][C:6]([OH:8])=[O:7].[CH2:11](OC(=O)CCCC(OCCC)=O)[CH2:12]C>>[CH2:11]([O:7][C:6](=[O:8])[CH2:5][CH2:4][CH2:3][CH2:2][C:1]([OH:10])=[O:9])[CH3:12]

Participants

Reactant 2

HCID 196Adipic Acid

HCID 74407Dipropyl glutarate

Product 1

HCID 122951-Ethyl hexanedioate

Procedure

Hexane dioic acid monoethyl ester was prepared from hexane dioic acid through steps (a) and (b) discussed above in example 1, step 2 for the preparation of (III).

Sources & evidence

ORD record: ord-f3270e93f5834c3f9429b910bb413032
Source dataset: uspto-grants-2014_03
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US08680288B2

Linked notes

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