1-Nonanethiol → 3-(1,3-Benzodioxol-5-yl)propyl nonyl disulfide

HRID 1195296

Reaction equation

HRID 1195296 reaction equation
[O:1]1[C:5]2[CH:6]=[CH:7][C:8]([CH2:10][CH2:11][CH2:12][SH:13])=[CH:9][C:4]=2[O:3][CH2:2]1.[CH2:14]([SH:23])[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]>>[CH2:14]([S:23][S:13][CH2:12][CH2:11][CH2:10][C:8]1[CH:7]=[CH:6][C:5]2[O:1][CH2:2][O:3][C:4]=2[CH:9]=1)[CH2:15][CH2:16][CH2:17][CH2:18][CH2:19][CH2:20][CH2:21][CH3:22]

Participants

3

Reactant 2

HCID 150771-NonanethiolHCID 190016193-(1,3-Dioxaindan-5-yl)propane-1-thiol

Product 1

HCID 571203063-(1,3-Benzodioxol-5-yl)propyl nonyl disulfideYield 56.1%

Procedure

6.2 g of the title compound was prepared from 10 g of 3-(1,3-benzodioxol-5-yl)propanethiol and 5 g of nonyl mercaptan as a colorless oil according to the same procedure as that described in Example 1.

Sources & evidence

ORD record
ord-cadb6a52c3d64e17a872ef7635c52dd8
Source dataset
uspto-grants-1992_05
Patent number
US05110956

Linked notes

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