Benzene, (3,3-diethoxy-1-propenyl)- → HCID 57296323, compound

Reaction equation

[Br:1][C:2]([CH:9]=[CH2:10])=[CH:3][O:4][Si](C)(C)C.[O:11]([CH:14](OCC)[CH:15]=[CH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[CH2:12][CH3:13]>>[Br:1][C:2](=[CH:3][CH2:4][CH:14]([O:11][CH2:12][CH3:13])[CH:15]=[CH:16][C:17]1[CH:22]=[CH:21][CH:20]=[CH:19][CH:18]=1)[CH:9]=[O:10]

Participants

Reactant 2

HCID 91340Benzene, (3,3-diethoxy-1-propenyl)-

HCID 53670473HCID 53670473, compound

Product 1

HCID 57296323HCID 57296323, compound

Procedure

One starts with 2.21 g of 2-bromo-1-trimethylsiloxybut-1,3-diene and 2.06 g of 3,3-diethoxyl-1-phenylprop-1-ene and proceeds in the same manner as in Example 3, except that the reaction is carried out for two hours.

Sources & evidence

ORD record: ord-5f02d14c75b34ef59a51a75e2003fa72
Source dataset: uspto-grants-1992_05
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05113007

Reaction notes

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