HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Benzothiazole-6-sulfonyl chloride → N-(2-Bromo-6-methyl-3-pyridyl)-6-benzothiazolesulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Benzothiazole-6-sulfonyl chloride | HCID 2795170 | — |
| Reactant | 2-Bromo-6-methylpyridin-3-amine | HCID 14418051 | — |
| Product | N-(2-Bromo-6-methyl-3-pyridyl)-6-benzothiazolesulfonamide | HCID 86622569 | 35% |
Reaction Steps
By working in a manner similar to that of Preparation VII, starting with 3-amino-2-bromo-6-methylpyridine and 6-benzothiazolesulfonyl chloride, the expected product is obtained in the form of a beige-colored paste (yield=35%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728002B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-547db05fcb5b4d15ad1859b271b0aa20 |
| Source note | uspto-grants-2010_06 |