HuagongsheHuagongshe Chemistry Print Report · For research reference only
Acetonitrile → HCID 178470380, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Acetonitrile | HCID 6342 | — |
| Reactant | 1-Naphthalenemethanamine | HCID 8355 | — |
| Reactant | Ethyl 2,3-dioxobutanoate | HCID 12260829 | — |
| Product | HCID 178470380 | HCID 178470380 | — |
Reaction Steps
A solution of 2,3-dioxobutyric acid ethyl ester, (Z)-2-oxime (3 g), 1-naphthalenemethylamine (3.26 g) in acetonitrile (45 ml) is refluxed for 10 hr to give a white precipitate. The solid is then collected, washed with acetonitrile and dried to yield 5-methyl-2-naphthalen-1-yl-3H-imidazole-4-carboxylic acid ethyl ester. LCMS 281.3 (M+1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728009B1 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-3f58c3e8254649fcb1cc5fa9783b5209 |
| Source note | uspto-grants-2010_06 |