Pentanal → 2-Propylhept-2-enal

HRID 1251033Notes

Reaction equation

HRID 1251033 reaction equation
[CH:1](=[O:6])[CH2:2][CH2:3][CH2:4][CH3:5]>O>[CH2:3]([C:2](=[CH:1][CH2:2][CH2:3][CH2:4][CH3:5])[CH:1]=[O:6])[CH2:4][CH3:5]

Participants

3

Reactant 1

HCID 8063Pentanal

Product 1

HCID 1187452-Propylhept-2-enal

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The nitrogen present in the crude product leaves the gas separator 8 via line 9 together with an azeotrope containing water, n-pentanal and the products. The stream was cooled (cooler and separator are not shown in FIG. 1). At the separator an organic phase and an aqueous phase were formed. The organic phase was passed to the product separator 11. The aqueous phase was discarded.

Workup

  1. temperatureThe stream was cooled (cooler and separator
  2. customAt the separator an organic phase and an aqueous phase were formed

Sources & evidence

ORD record
ord-c00c92fdb88a48079e4846c4b71582c9
Source dataset
uspto-grants-2002_01
Patent number
US06340778B1

Reaction notes

Loading…