HuagongsheHuagongshe Chemistry Print Report · For research reference only
N,N'-Dimethylethylenediamine → 1-(5,6-Diphenyl-pyridin-2-yl)-propan-1-one
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N,N'-Dimethylethylenediamine | HCID 8070 | — |
| Reactant | Ethyl 5,6-diphenylpyridine-2-carboxylate | HCID 14789610 | — |
| Reactant | Triethylaluminum | HCID 16682930 | — |
| Solvent | Toluene | HCID 1140 | — |
| Product | 1-(5,6-Diphenyl-pyridin-2-yl)-propan-1-one | HCID 25033167 | — |
Reaction Steps
Following General Procedure O, ethyl 5,6-diphenylpyridine-2-carboxylate (Compound 21, 267 mg, 0.81 mmol) in toluene (5 ml), N,N′-dimethylethylenediamine (DMEDA, 85 mg, 0.97 mmol) and triethylaluminum (2.6 ml, 2.64 mmol, 1 M in hexane) were reacted to give the title compound as a yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07728014B2 |
| Source dataset | uspto-grants-2010_06 |
| ORD ID | ord-17477629f93f4d5e92fb9a72fe881df8 |
| Source note | uspto-grants-2010_06 |