2-Butyl-n-octan-1-amine → HCID 178443254, compound

HRID 1261707

Reaction equation

HRID 1261707 reaction equation
[CH2:1]([CH:11]([CH2:63][CH2:64][CH2:65][CH2:66][CH2:67][CH2:68]CCCCCC)[CH2:12][N:13]=[C:14]([C:16]1[C:25]2[C:24]([C:26]([OH:28])=[O:27])=[C:23]([Br:29])[C:22]([Br:30])=[C:21]([C:31]([OH:33])=[O:32])[C:20]=2[C:19]([C:34](=[N:36][CH2:37][CH:38]([CH2:51][CH2:52][CH2:53][CH2:54]CCCCCC)[CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH2:44]CCCCCC)[OH:35])=[C:18]([Br:61])[C:17]=1[Br:62])[OH:15])[CH2:2][CH2:3][CH2:4]CCCCCC.C(C(CCCCCC)CN)CCC>>[CH2:51]([CH:38]([CH2:39][CH2:40][CH2:41][CH2:42][CH2:43][CH3:44])[CH2:37][N:36]=[C:34]([C:19]1[C:20]2[C:21]([C:31]([OH:33])=[O:32])=[C:22]([Br:30])[C:23]([Br:29])=[C:24]([C:26]([OH:28])=[O:27])[C:25]=2[C:16]([C:14](=[N:13][CH2:12][CH:11]([CH2:1][CH2:2][CH2:3][CH3:4])[CH2:63][CH2:64][CH2:65][CH2:66][CH2:67][CH3:68])[OH:15])=[C:17]([Br:62])[C:18]=1[Br:61])[OH:35])[CH2:52][CH2:53][CH3:54]

Participants

3

Reactant 2

HCID 186732842-Butyl-n-octan-1-amineHCID 178442862HCID 178442862, compound

Product 1

HCID 178443254HCID 178443254, compoundYield 25%

Procedure

The same synthetic method for compound 22 was used except using 2-butyloctyl amine instead of 2-decyltetradecyl amine, and the yield was 25% (calculated based on TBNDA as a starting material).

Sources & evidence

ORD record
ord-5959b412fd434e02b66262cb6d689aab
Source dataset
uspto-grants-2013_06
Patent number
US08471021B2

Linked notes

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