Dimethylamine → HCID 70009801, compound
Reaction equation
Cl[CH:2]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:15]3[CH2:16][CH2:17][C:18]4[NH:19][C:20](=[O:23])[CH:21]=[CH:22][C:13]([C:14]=43)=[CH:12][N:11]=2)=[CH:6][CH:5]=1)[CH3:3].[CH3:24][NH:25][CH3:26]>>[CH3:24][N:25]([CH3:26])[CH:2]([C:4]1[CH:9]=[CH:8][C:7]([C:10]2[N:15]3[CH2:16][CH2:17][C:18]4[NH:19][C:20](=[O:23])[CH:21]=[CH:22][C:13]([C:14]=43)=[CH:12][N:11]=2)=[CH:6][CH:5]=1)[CH3:3]Participants
3
Conditions
- Temperature
- 80 °C
Procedure
This compound was prepared from intermediate 245b and dimethylamine according to the procedure described in Example 171, with the exception of heating to 80° C. Received 69 mg (77%)
Sources & evidence
- ORD record
- ord-19009312ab88405488fa4711c41740cb
- Source dataset
- uspto-grants-2003_04