Ethanol → HCID 46311348, compound

Reaction equation

[CH2:1]([O:8][C:9]1C=CC(Br)=CC=1C(C)(C)C)[C:2]1C=CC=CC=1.[F:20][C:21]1[C:26]([F:27])=[CH:25][C:24](Br)=[CH:23][C:22]=1[OH:29].CC[OH:32]>>[CH2:1]([O:8][C:9](=[O:32])[C:24]1[CH:23]=[C:22]([OH:29])[C:21]([F:20])=[C:26]([F:27])[CH:25]=1)[CH3:2]

Participants

Reactant 3

HCID 702Ethanol

HCID 27733075-Bromo-2,3-Difluorophenol

HCID 184546141-Benzyloxy-4-bromo-2-tert-butyl-benzene

Product 1

HCID 46311348HCID 46311348, compound

Procedure

The title compound was synthesized by substituting 1-benzyloxy-4-bromo-2-tert-butyl-benzene in Example 47C with 2,3-difluoro-5-bromophenol in EtOH. MS (DCI) m/z 220 (M+NH4)+.

Sources & evidence

ORD record: ord-a64800570a184224bd75fed74afbfbad
Source dataset: uspto-grants-2007_04
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US07205409B2

Reaction notes

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