HuagongsheHuagongshe Chemistry Print Report · For research reference only
Chloride → 2-Methyl-3,4,6-trifluorobenzoyl chloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Chloride | HCID 312 | — |
| Reactant | 2-Methyl-3,4,6-trifluorobenzoic acid | HCID 10130305 | — |
| Product | 2-Methyl-3,4,6-trifluorobenzoyl chloride | HCID 15007607 | — |
Reaction Steps
To 2-methyl-3,4,6-trifluorobenzoic acid (3.2 g) is added thiony chloride (7 ml) and the mixture is refluxed for 1 hour. After concentrating, 2-methyl-3,4,6-trifluorobenzoyl chloride (3.3 g) is obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05723648 |
| Source dataset | uspto-grants-1998_03 |
| ORD ID | ord-141b4f862c4146f6950ca566cd749152 |
| Source note | uspto-grants-1998_03 |