2-((Benzylamino)methyl)phenol → HCID 22665691, compound

Reaction equation

[CH2:1]([N:8]=[CH:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:11]=1[OH:18])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[BH4-].[Na+].C(NCC1C=CC=CC=1O)C1C=CC=CC=1>>[CH2:1]([NH:8][CH2:9][C:10]1[CH:15]=[C:14]([O:16][CH3:17])[CH:13]=[CH:12][C:11]=1[OH:18])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

Participants

Reactant 3

HCID 4083602-((Benzylamino)methyl)phenol

HCID 4311764Sodium borohydride

HCID 1355950552-(Benzylimino-methyl)-4-methoxy-phenol

Product 1

HCID 22665691HCID 22665691, compound

Procedure

This compound was prepared from 1.0 g of 2-(benzylimino-methyl)-4-methoxy-phenol and 0.18 g of sodium borohydride using the procedure described 64b. Yield: 1.0 g (oil), EI-MS: 243 (M+).

Sources & evidence

ORD record: ord-af25a66f923844b3b7d9a98a1631c429
Source dataset: uspto-grants-2002_09
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06444672B1

Reaction notes

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