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Glycidyl methacrylate → 2,3-Epithiopropyl methacrylate

HRID 128151
Notes
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Reaction equation

HRID 128151 reaction equation
[C:1]([O:6][CH2:7][CH:8]1O[CH2:9]1)(=[O:5])[C:2]([CH3:4])=[CH2:3].NC(N)=[S:13]>O.C(O)C>[C:1]([O:6][CH2:7][CH:8]1[S:13][CH2:9]1)(=[O:5])[C:2]([CH3:4])=[CH2:3]
ParticipantsProcedureSources & evidenceReaction notes

Participants

5

Reactant 2

HCID 7837Glycidyl methacrylateHCID 2723790Thiourea

Product 1

HCID 1029412,3-Epithiopropyl methacrylate

Reagents, catalysts & solvents 2

HCID 702EthanolSolventHCID 962WaterSolvent

Procedure

Glycidyl methacrylate corresponding to the formula: ##STR10## is reacted with thiourea corresponding to the formula: ##STR11## at ambient temperature in a mixture of water and ethanol. The reaction gives 2,3-epithiopropyl methacrylate corresponding to the formula: ##STR12##

Sources & evidence

ORD record
ord-c5710a8a6cf24c09a6f08cca881611f9
Source dataset
uspto-grants-1981_03
DOI
10.6084/m9.figshare.5104873.v1
Patent number
US04259162

Reaction notes

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On this pageParticipantsProcedureSources & evidenceReaction notes