Acetyl chloride → HCID 68140100, compound

Reaction equation

[CH2:1]([CH2:4][NH:5][CH2:6][CH:7]([C:9]1([OH:21])[CH2:14][CH2:13][CH2:12][CH2:11][CH:10]1[C:15]1[CH:20]=[CH:19][CH:18]=[CH:17][CH:16]=1)[CH3:8])[CH:2]=[CH2:3].[C:22](Cl)(=[O:24])[CH3:23]>>[C:22]([O:21][C:9]1([CH:7]([CH3:8])[CH2:6][NH:5][CH2:4][CH2:1][CH:2]=[CH2:3])[CH2:14][CH2:13][CH2:12][CH2:11][CH:10]1[C:15]1[CH:16]=[CH:17][CH:18]=[CH:19][CH:20]=1)(=[O:24])[CH3:23]

Participants

Reactant 2

HCID 6367Acetyl chloride

HCID 21519253HCID 21519253, compound

Product 1

HCID 68140100HCID 68140100, compound

Procedure

The procedure of Example I(c) is followed using 4.8 g of 1-(2-Allylmethylamino-1-methylethyl)-2-phenylcyclohexanol and 13 ml acetyl chloride to give 3.2 g pure product.

Sources & evidence

ORD record: ord-7532307eb2774f8ea79f1b48501f1a90
Source dataset: uspto-grants-1976_08
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US03974157

Reaction notes

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