HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromophenol → p-Bromo-(1-methoxyethoxy)benzene
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromophenol | HCID 7808 | — |
| Reactant | Methyl vinyl ether | HCID 7861 | — |
| Product | p-Bromo-(1-methoxyethoxy)benzene | HCID 22908633 | 90% |
Reaction Steps
Using p-bromophenol (17.3 g, 0.1 mole) and methyl vinyl ether (14.0 g, 0.2 mole), the reaction was carried out in the same manner as described in Synthesis Example 1, (1), and the crude oil (24 g) was purified by distillation under reduced pressure to afford 20.8 g of p-bromo-(1-methoxyethoxy)benzene as a pale yellow oil having a boiling point 89-90° C./2 mmHg.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05468589 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-24808c6fb6474ee0bab5996c316c4c25 |
| Source note | uspto-grants-1995_11 |