HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Nitrophenethyl alcohol → 4-Aminophenethyl alcohol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Nitrophenethyl alcohol | HCID 7494 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 4-Aminophenethyl alcohol | HCID 66904 | 87.7% |
Reaction Steps
A slurry of 5 g of 4-nitrophenethyl alcohol, 0.58 g of 10% Pd on carbon in 50 mL of absolute ethanol was shaken overnight under 50 psi of H2. The mixture was filtered and concentrated to yield 3.6 g of 4-(2-hydroxyethyl) aniline, mp 101°-102° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05468641 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-84bb3790b7794231954cde8825badf3b |
| Source note | uspto-grants-1995_11 |