Sulfuric Acid → HCID 14852523, compound

HRID 129664

Reaction equation

HRID 129664 reaction equation
[OH:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([OH:8])=[O:7])=[C:4]([CH3:11])[CH:3]=1.S(=O)(=O)(O)O.[CH2:17](O)[CH:18]=[CH2:19]>>[OH:1][C:2]1[CH:10]=[CH:9][C:5]([C:6]([O:8][CH2:19][CH:18]=[CH2:17])=[O:7])=[C:4]([CH3:11])[CH:3]=1

Participants

4

Reactant 3

HCID 1118Sulfuric AcidHCID 7858Allyl AlcoholHCID 684754-Hydroxy-o-toluic acid

Product 1

HCID 14852523HCID 14852523, compoundYield 76%

Procedure

In a manner analogous to Example 1(a), 5.34 g (32 mmoles) of 4-hydroxy-2-methyl benzoic acid treated at 100° C. for 12 hours with 50 ml of allyl alcohol and 1.5 ml of concentrated sulfuric acid, give 4 g (76% yield) of the expected ester having a melting point of 76°-77° C.

Sources & evidence

ORD record
ord-c4ecc55df621403087197065d9dc476a
Source dataset
uspto-grants-1995_11
Patent number
US05468897

Linked notes

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