HuagongsheHuagongshe Chemistry Print Report · For research reference only
L-(+)-Cysteine → HCID 14881540, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | L-(+)-Cysteine | HCID 5862 | — |
| Reactant | Bis(2-pyridyl) ketone | HCID 88065 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 14881540 | HCID 14881540 | 11% |
Reaction Steps
A mixture of 3.68 g of di-2-pyridyl ketone, 2.42 g of L-cysteine, 25 ml of ethanol was refluxed for 3.5 hours. After allowing the mixture to cool, the insoluble matter was filtered off, and the filtrate was concentrated to dryness under reduced pressure. The residue was washed in sequence with ethyl acetate and ether to give 0.63 g of 2,2-di(2-pyridyl)-thiazolidine-4-carboxylic acid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05470851 |
| Source dataset | uspto-grants-1995_11 |
| ORD ID | ord-fbee9d5e5b41400f9f3691bf051546d4 |
| Source note | uspto-grants-1995_11 |